Hydrothermal Reactor

High Pressure Oxygen Tube Furnace (HIP) with 20mm ID up to 1100C @ 700PSI - OTF-1200X-HP-55-UL

High Pressure Oxygen Tube Furnace (HIP) with 20mm ID up to 1100C @ 700PSI - OTF-1200X-HP-55-UL

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Product Name High Pressure Oxygen Tube Furnace (HIP) with 20mm ID up to 1100C @ 700PSI - OTF-1200X-HP-55-UL
Sale Price Call for Price
Product Code OTF-1200X-HP-55-UL
Quantity 수량증가수량감소
상품 옵션
 
  • High Pressure Tube Furnace with 20mm ID. Super-alloy Tube up to 1100C @ 700PSI- OTF1200X-HP-55-UL
  • OTF-1200X-HP-55-UL is a split tube furnace with CE/UL/CSA certified electrical components.    Ni based super-alloy tube (55 mm O.D x 20 mm I.D x 600 mm L) and flanges/valves.    It is designed for using at high pressure (7 MPa) up to 1100°C under oxidizing and inert gas atmosphere to process special compound.    It is a ideal furnace to use for preparing new materials under high pressure, and also can be use as mini HIPto treat metallic sample. ( Laptop is included since 9/10/15 )
  •  SPECIFICATIONS
  • Furnace Structure
  • Double layer steel casing with air cooling.
    High purity fibrous alumina insulation for max. energy saving.
    Aluminum heat sink on processing tube to ensure pressure flange and fitting < 80°C
    All Elctric parts are UL cerified and ready to pass TUV, CSA and UL cerificate
  • Power
  • 2.5 KW
  • Voltage
  • AC 208 - 240V Single Phase, 50/60 Hz
  • Max. Temperature
  • 1100°C
  • Max. Heating Rate
  • <= 30°C/min
  • Material and Size of Pressure Vessel 

  • Special Ni based Super-alloy : ( Waspaloy or equivalent )
    55 mm O.D x 20 mm I.D. x 580 mm Length
    1/4BSPP fitting is installed in end of flange, and 1/4" high pressure stainless steel pipe shall be connected to the fitting.
    Please click picture below to see detail of pressure vessel

    Exterior

    Interior
    Attention : Processing Tube is consumable part, you can click picture below to order replacement or spare one.
    Copper Gasket  Size : 27.2 mm O.D x 20 mm I.D x 2 mm thickness
    Optional torque wrench is available here to avoid overtighten the flange bolts.    The suitable tightening torque for 55 OD x 20 ID x 580 L (mm) is 40 foot pound.
     
  • Compatible Gas and crucible
  • O2 and inert gases such as N2, Ar and He
     
    Note

    ○  A small quartz or Alumina boat may be needed to contain sample inside chamber.    Please click link below to order separately
    ○  For best result, you may use gold or nickel foil wrapping sample and put in the crucible boat to avoid contamination

     
  • Heating Zone length
  • 250 mm ( single zone )
  • Temperature Uniformity
  • Constant Temperature Zone length

    ○  50mm within +/-1°C and 70mm within +/-2°C in

    click the picture below to view the details of the Temperature Distribution Curve and Testing :

    Temp. Control ( left meter )
  • Temperature controller
  • MET certified 30 programmable segments for precise control of heating rate, cooling rate and dwell time.
    Built in PID Auto-Tune function with overheating & broken thermocouple broken protection.
    Over temperature protection and alarm allows for operation without attendant(s).
    +/- 1 ºC temperature accuracy.
  • PC Control
  • A MTS-03  control  software is included for controlling and displaying temperature and pressure by PC at remote location. A brand new labtop with pre-installed & tested software is included for immediate use
    Please don't try to buy furnace without computer because laibility issues
     
  • Pressure Sensor and Display
  • Pressure measurement range : 0~25Mpa
    The pressure sensor is installed in the flange.    The pressure will be displayed in the pressure controller in the front panel of furnace.
    The alarm system is built in the pressure controller which allow user to set up the high and low limit point of pressure.    When the measuring pressure exceed limit point, the alarm strobe and whistle will be activated for warning.
    Optional : Adjustable High Pressure Relief Valve 1000 - 10,000 PSI ( 7 - 70 Mpa ),  click picture below right to order.

    Pressure Display(right))

    flange assembly

    High pressure Relief Valve 
  • Pressure Fitting
  • One Super-alloy flanges is included.
    One Aluminum heat radiators are installed in front of flange to keep flange below 100oC
    One high pressure valves are installed with flanges
    One Pressure meter installed to one of valve
    Note & warning :
     Optional : You may order four Pt wire ( 0.35 mm dia ) feedthrough to install with the furnace for measure material electric conductivity under high pressure upto 1100oC at extra cost (    )
     
    The safety pressure relief valve is available to be installed at the downstream side.    Please click here for details.
  • Working Pressure
    vs
    temperature
  • Allowable pressure (sf = 2) Heating temperature
    Max. 4000 PSI (30 Mpa) 800°C
    Max. 2600 PSI (18 Mpa) 900°C
    Max. 1320 PSI (9 Mpa) 1000°C
    Max. 870 PSI (6 Mpa) 1100°C
    The allowable pressure is calculated based on Barlow's formula. S = yield strength. Safety factory= 2 Click to download  GH747 nickel based alloy datasheet
    Warning

    ○  Please set up pressure alarm point in digital pressure display before operation
    ○  Must install a pressure regulator on gas cylinder to increase pressure gradually.

  • Heating Element
  • Fe-Cr-Al Alloy doped by Mo
  • Dimensions
  • 550 x 380 x 520mm
  • Net Weight
  • About 45Kg
  • Shipping package Dimensions
  • 45 x 45 x 35 inch
  • Shipping weight
  • 200lbs
  • Warranty
  • One year limited warranty (Consumable parts such as o-rings and heating elements are not covered by the warranty, please order the replacement at related products below.)
  • Certificate
  • CE Certified
    All electric components ( >24V) are UL / MET / CSA certified
    The furnace is ready to pass TUV(UL61010) or CSA certification at extra cost. ( please click marks below to learn details )
     
     
  • Operation Instructions
  • Safety Notes

    pics show Ni based Super-alloy ( Waspaloy or equivalent) processing tube under overpressure test
  • Ni based Super-alloy ( Waspaloy or equivalent) is a reliable processing tube which can be used under high temperature and high pressure.    It has excellent ductility and tensile property so only creep deformation happens under overpressure destruction test and following by a crack formed (usually at the hot zone at the center of tube) to release the pressure.    Brittle fracture won’t happen in the overpressure destruction test which means no tube explosion will happen under overpressure of inert gas or safe gas or under other accidents causing overpressure of inert gas or safe gas
    Please never use ordinary SS tube to connect to gas-inlet for using > 5Mp pressure, whcih may cause tube exploded.
    Attention : for the use with flammable, toxic or corrosive gases, you must contact MTI engineering group for the consultation to know all the prerequisites and precautionary measures.
    Attention : A two stage pressure regulator must be installed on gas cylinder to limit the pressure to below 3 PSI for safe operation.    Click here to learn the installation of a gas regulator. 
    Do not over tightening the flange screws as this may cause permenent damages to the flange or screws.    Please refer to  the instructions about proper torque for installing CF flange bolts.    We recommend you use torque wrench  to tighten the screws with the flange.