High Pressure & Vacuum Tube Furnace

1100°C Eight Zone High Pressure Super-Alloy Tube Furnace with Gas Flow & Pressure Control System - OTF-1200X-VIII-80-GF

1100°C Eight Zone High Pressure Super-Alloy Tube Furnace with Gas Flow & Pressure Control System - OTF-1200X-VIII-80-GF

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Product Name 1100°C Eight Zone High Pressure Super-Alloy Tube Furnace with Gas Flow & Pressure Control System - OTF-1200X-VIII-80-GF
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Product Code OTF-1200X-VIII-80-GF
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OTF-1200X-HP-VIII-80-GF is a high-pressure tube furnace with eight heating zones and pressure control system. The processing tube is made of Ni-based superalloy (50 mm ID x 2000mm L) which can withstand high pressure (oxygen or inert gases) under 1100°C max. Its pressure control system can maintain a stable pressure during the heating process which is critical for processing Fe-based superconductive material, or new generation oxide ceramics.


SPECIFICATIONS


Furnace & Power


  •      •  Splittable Eight heating zone tube furnace with air cooling layer
  •      •  High-quality fibrous insulation and reflective coating for max. energy saving.
  •      •  Power:  208 - 240VAC 50/60Hz, Single Phase, 9.6KW max. (circuit breaker which is rated
           @ 60amps or higher is recommended)



Heating Zone

  •      •  Eight heating zones:   150mm / zone
  •      •  Total heating zone length: 1200mm
  •      •  Constant temp. zone: 900mm ±5°C

 
   Working Temperature

  •      •  1100°C max.for < 1hr  
  •      •  1000°C for continuous
  •      •  Heating rate: ≤10°C/min


Temperature Control



    •      •  Touch screen temperature controller is built in a control station which provides individual controls
              over the eight heating zones
    •      •  Each channel is with PID auto-tuning, up to 30 segments programmable
    •      •  Built-in overheating & thermocouple failure protection.
    •      •  +/- 1 ºC temperature accuracy.


    Thermocouple




    •      •  Omega 3mm OD K Type
       with high-temperature (220°C) connector
    •      •  Total 8 TCs, one for each zone

    Process Vessel



    •      •  The pressure vessel is made of Nickel-based superalloy GH747
              (
      Click to download GH747 nickel-based alloy datasheet)
    •      •  Vessel size: OD 85 x  ID 50 x  Length 2000 (mm)
    •      •  Optional: torque wrench is available here to avoid over-tighten the flange bolts.
             Please click the image on the left to order.
    •      •  Warning: Never put a sample inside tube directly without crucible or isolated foil to avoid
              sample react with tube alloy.



    Working Pressure

    •      •  20 Mpa max. at  <800°C
    •      •  13 Mpa max. at <900°C
    •      •  6   Mpa max. at <1000°C
    •      •  4   Mpa max. at <1100°C
    •      •  Never heat up above 1200°C


    Working Gases

    •      •  Inert gas and oxygen
    •      •  No hydrogen or any flammable gas


    Flange and  Fitting





    •      •  Two CF type flanges are weld with female 1/4"NPT fitting to connect high-pressure tube
    •      •  2 pcs Copper o-rings are included  ( spare copper O-ring is available as consumable )
                    

    Gas Flow & Pressure Control System



    •      •  Gas flow and pressure control system is built in a heavy-duty mobile table under the furnace and
              safety frame
    •      •  Two pressure sensors and digital displays are installed to monitor the pressure for gas inlet and
              furnace tube
    •      •  One high-pressure mass flow controller is installed at the gas outlet to control gas flow rate with
               max. 10Mpa working pressure and 500 SCCM flow rate
       
    •      •  Pressure relief valves are installed to ensure safety. The valve will release gas when the pressure
               reaches the setting point.



    Dimension & Weight

    •      •  Dimension:  26000mmL*700mmW*947mmH (furnace); 1100mmL*600W*1200mmH (control consol)
    •      •  Net weight:  480 kg

    Operation Instruction

    Compliance and Warranty

    •      •  All electric components 
             ( >24V) are UL or MET listed, and ready to pass TUV, UL or CSA certificate on feild at extra cost

                                     
                     ( click mark to learn what is )

    •      •  One year limited warranty for lifetime support


    Application Notes

    •      •  Hytort Application, or named Hydroretorting of Shale Oil
       is a process developed by IGT to double the yield
              of shale oil and hydrocarbon gases. MTI High-Pressure furnaces with Ni-based superalloy tube is an
              ideal tool for conducting related experiments. Please click underlined to view research paper.


    Safety Notes

    •      •  Ni-based Superalloy ( Waspaloy or equivalent) is a reliable processing tube which can be used under
              high temperature and high pressure.. It has excellent ductility and tensile property so only creep
              deformation happens under overpressure destruction test and following by a crack formed (usually at
             the hot zone at the center of tube) to release the pressure. Brittle fracture won’t happen in the
             overpressure destruction test which means no tube explosion will happen under an overpressure of
             inert gas or safe gas or under other accidents causing overpressure .


                       

                     Above pics show Ni-based Super-alloy
                     ( Waspaloy or equivalent) processing tube under overpressure test

    •      •  Attention: For the use with flammable, toxic or corrosive gases, you must contact MTI
              engineering group for the consultation to know all the prerequisites and precautionary
              measures.

    •      •  Attention: A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to
              below 3 PSI for safe operation.
      Please click here to learn how to install the gas regulator.