Ultrasonic Spray Pyrolysis Furnace for Nano/Core-S

1200°C Max. Ultrasonic Spray Pyrolysis 3-Zone Furnace for Nano Particles Synthesis - OTF-1200X-III-PGEP

1200°C Max. Ultrasonic Spray Pyrolysis 3-Zone Furnace for Nano Particles Synthesis - OTF-1200X-III-PGEP

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Product Name 1200°C Max. Ultrasonic Spray Pyrolysis 3-Zone Furnace for Nano Particles Synthesis - OTF-1200X-III-PGEP
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Product Code OTF-1200X-III-PGEP
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상품 옵션
Personalization(Upgrade to Eurotherm Temp. Controller)

Personalization

 
OTF-1200X-PGEP is a versatile ultrasonic spray furnace system designed for nano, core-shell structured particle synthesis.  The system consists of three major modules: 1.7MHz ultrasonic enhanced bubbler, 1200ºC Max. 3 zone heating tube furnace, and Electrostatic Precipitator.   The processing steps of a particle includes aerosol generation, thermal decomposition, and nanopowder collection. Such a system enables advanced synthetic method that provides control over particle size, morphology, nano/microstructure.


SPECIFICATIONS


System Structure





  •      •  Aerosol Generation: 1.7 MHz Ultrasonic Enhanced Bubbler can "evaporate" catalyst liquid with
            literally no heat generated.
    A stainless steel liquid collector connects inline with the ultrasonic bubble
            can prevent condensing liquid from streaming into the furnace tube chamber.
  •      •  Thermal Decomposition:  three-zone ( 900mm length ) tube furnace can be heated up to 1200C
             maximum to pass the droplets flux across the temperature and atmosphere regulated firing zone,
             chemical, and physical conversion processes proceed.  
  •      •  Nanopowder Collection: 30KV  electrostatic precipitator (700 ml ) can effectively collect nano-size
             particles from the carrier gas flow
  •      •  The furnace can be tilted to avoid liquid flow back  atomizing tank


Tube Furnace -

Thermal Decomposition





Voltage & Power

  •      •  Single Phase, 208V~240V AC, 50/60 Hz   (30A breaker required)
  •      •  Max. 7 KW

 
   Working Temperature

  •      •  1100oC  continuous
  •      •  1200 oC  Max. < 1 hours

   Max. Heating / Cooling Rate< 20oC / min

Heating Zone & Constant Temperature Zone

  •      •  Three heating zone, 300+ 300 + 300 mm ( 900mm L total)
  •      •  Constant temperature zone:   600 mm with +/- 2oC
            ( if 3 zone at same )


    Heating Elements
  •      •  Fe-Cr-Al Alloy doped by Mo

Temperature Controller



  •      •  Three digital temperature controllers with 30 programmable
            segments for precise control of heating rate, cooling rate and dwell
            time.
  •      •  Built-in over-temperature alarm and protection allow for operation
  •      •  +/- 1 ºC temperature accuracy.
  •      •  RS485 Communication Port.
  •      •  Precision Eurothermo controller is available with +/- 0.1 oC
            accuracy



Processing Tube

  •      •  O
    ne fused quartz tube is included with ID 20.5 x OD 25 mm x L
             1400 ( mm)


Sealing Flanges

& Fittings


  •      •  Left side sealing KF flange which connects atomizing bubbler and
            1" quartz tube with vacuum gauge.
  •      •  Right side KF flang connects to the electrostatic precipitator.

                   Left             
                   Right
  


Aerosol Generation


     

Ultrasonic atomizing bubbler




  •      •  220VAC, 1.7 MHz Ultrasonic Generator
  •      •   Ultrasonic power is adjustable with 8 levels
  •      •  316 Stainless Steel liquid container with a fluoropolymer sealing
             ring
  •      •  The continuous or timed mode can be set. For timed mode, time
             can be adjusted from 30 minutes to 180 minutes.
  •      •  A liquid injection pump is equipped with a 60 ml plastic syringe.
            The speed range for the liquid injection pump is 0.004 ml/min - 70
            ml/min
  •      •  A floating flow meter is included to control the carrier gas flow rate
            within 0-200 SCCM.
  •      •  vA mass flow controller (MFC) is optional to precisely control the
            flow rate.



Nanopowder Collection





High Voltage Supply



  •      •  AC 220V 50/60Hz, 30 W Max. power consumption
  •      •  Digital Voltmeter and Current meter, 30KV, 1.0 mA max.
  •      •  Output voltage and current can be set by using knobs on the front
            panel and read from the digital display
  •      •  Built-in Arc Protection Circuit


Electrostatic Precipitator




  •      •  KF25 quick clamp and flange enables the quick coupling to the
            furnace processing tube
  •      •  1/4" gas outlet built-in
  •      •  Another KF25 port is built-in with the collector to connect the
            vacuum pump, which is required, but not included
  •      •  PEFE plates are installed on top and bottom to insulate high
             voltage electrodes
  •      •  Adjustable supports keep the collector leveled with the furnace tub

Net Weight~150Kg
Dimensions( click the picture to see details)
WarrantyOne year limited manufacturer warranty with lifetime support (consumable parts such as furnace liner, processing tubes, and O-rings are not covered by the warranty, please order replacements at related products below).

Laptop, software & WiFi Control (Optional)

   

  •      •  Brand new laptop with Microsoft Window 10 and Microsoft Office
            2013 (30 days free trial) for immediate use.
  •      •  Labview Based Temperature Control System (EQ-
            MTS01
    )
     enables the user to edit temperature profile, manage
            heat-treatment recipe, record and plot data for MTI furnaces.


Compliance

   


  •      •  CE Certified
  •      •  NRTL or CSA certification (UL61010) is available upon request at
             extra

Application Notes

 

  •      •  A two-stage pressure regulator must be installed on the gas
            cylinder to limit the pressure to below 3 PSI for safe
            operation.
     
    Click here to learn the installation of a gas regulator.
  •      •   Please tilt furnace in 10 - 15 degrees to avoid liquid back to
             atomizing bubbler
  •      •  It is the customer responsibility to achieve the ideal parameter for
            particle size. Usually, the liquid injection rate and carrier gas flow
            rate has an important influence on particle size.
  •      •  The SEM picture left is SnO2 particle ( ~ 500 nm - 5 um) generated
             by the equipment via Stannic chloride solution at 800oC



Operation Video & Instructions