System Structure
| • Aerosol Generation: 1.7 MHz Ultrasonic Enhanced Bubbler can "evaporate" catalyst liquid with literally no heat generated. A stainless steel liquid collector connects inline with the ultrasonic bubble can prevent condensing liquid from streaming into the furnace tube chamber. - • Thermal Decomposition: three-zone ( 900mm length ) tube furnace can be heated up to 1200C
maximum to pass the droplets flux across the temperature and atmosphere regulated firing zone, chemical, and physical conversion processes proceed. - • Nanopowder Collection: 30KV electrostatic precipitator (700 ml ) can effectively collect nano-size
particles from the carrier gas flow - • The furnace can be tilted to avoid liquid flow back atomizing tank
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Tube Furnace - Thermal Decomposition
| Voltage & Power | • Single Phase, 208V~240V AC, 50/60 Hz (30A breaker required)- • Max. 7 KW
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Working Temperature | • 1100oC continuous- • 1200 oC Max. < 1 hours
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Max. Heating / Cooling Rate | < 20oC / min
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Heating Zone & Constant Temperature Zone | • Three heating zone, 300+ 300 + 300 mm ( 900mm L total)- • Constant temperature zone: 600 mm with +/- 2oC
( if 3 zone at same )
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Heating Elements
| - • Fe-Cr-Al Alloy doped by Mo
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Temperature Controller
| • Three digital temperature controllers with 30 programmable segments for precise control of heating rate, cooling rate and dwell time.- • Built-in over-temperature alarm and protection allow for operation
- • +/- 1 ºC temperature accuracy.
- • RS485 Communication Port.
- • Precision Eurothermo controller is available with +/- 0.1 oC
accuracy
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Processing Tube | • One fused quartz tube is included with ID 20.5 x OD 25 mm x L 1400 ( mm)
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Sealing Flanges & Fittings
| • Left side sealing KF flange which connects atomizing bubbler and 1" quartz tube with vacuum gauge.- • Right side KF flang connects to the electrostatic precipitator.
Left Right
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Aerosol Generation
| Ultrasonic atomizing bubbler
| • 220VAC, 1.7 MHz Ultrasonic Generator- • Ultrasonic power is adjustable with 8 levels
- • 316 Stainless Steel liquid container with a fluoropolymer sealing
ring - • The continuous or timed mode can be set. For timed mode, time
can be adjusted from 30 minutes to 180 minutes. - • A liquid injection pump is equipped with a 60 ml plastic syringe.
The speed range for the liquid injection pump is 0.004 ml/min - 70 ml/min - • A floating flow meter is included to control the carrier gas flow rate
within 0-200 SCCM. - • vA mass flow controller (MFC) is optional to precisely control the
flow rate.
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Nanopowder Collection
| High Voltage Supply
| • AC 220V 50/60Hz, 30 W Max. power consumption- • Digital Voltmeter and Current meter, 30KV, 1.0 mA max.
- • Output voltage and current can be set by using knobs on the front
panel and read from the digital display - • Built-in Arc Protection Circuit
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Electrostatic Precipitator
| • KF25 quick clamp and flange enables the quick coupling to the furnace processing tube- • 1/4" gas outlet built-in
- • Another KF25 port is built-in with the collector to connect the
vacuum pump, which is required, but not included - • PEFE plates are installed on top and bottom to insulate high
voltage electrodes - • Adjustable supports keep the collector leveled with the furnace tub
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Net Weight | ~150Kg |
Dimensions | ( click the picture to see details) |
Warranty | One year limited manufacturer warranty with lifetime support (consumable parts such as furnace liner, processing tubes, and O-rings are not covered by the warranty, please order replacements at related products below). |
Laptop, software & WiFi Control (Optional)
| • Brand new laptop with Microsoft Window 10 and Microsoft Office 2013 (30 days free trial) for immediate use.- • Labview Based Temperature Control System (EQ-
MTS01) enables the user to edit temperature profile, manage heat-treatment recipe, record and plot data for MTI furnaces.
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Compliance
| • CE Certified- • NRTL or CSA certification (UL61010) is available upon request at
extra
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Application Notes
| • A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to below 3 PSI for safe operation. Click here to learn the installation of a gas regulator.- • Please tilt furnace in 10 - 15 degrees to avoid liquid back to
atomizing bubbler - • It is the customer responsibility to achieve the ideal parameter for
particle size. Usually, the liquid injection rate and carrier gas flow rate has an important influence on particle size. - • The SEM picture left is SnO2 particle ( ~ 500 nm - 5 um) generated
by the equipment via Stannic chloride solution at 800oC
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Operation Video & Instructions |
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