Ultrasonic Spray Pyrolysis Furnace for Nano/Core-S

Tube Furnace with 2.4MHz Ultrasonic Spraying and Electrostatic Precipitator upto 1800°C for Special -Particle Formation - GSL-1800X-PGEP

Tube Furnace with 2.4MHz Ultrasonic Spraying and Electrostatic Precipitator upto 1800°C for Special -Particle Formation - GSL-1800X-PGEP

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Product Name Tube Furnace with 2.4MHz Ultrasonic Spraying and Electrostatic Precipitator upto 1800°C for Special -Particle Formation - GSL-1800X-PGEP
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Product Code GSL-1800X-PGEP
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GSL-1800X-PGEP is a versatile synthetic system designed for nanostructured oxide materials. Three major modules (Ultrasonic Enhanced Bubbler, Tube Furnace, and Electrostatic Precipitator) are employed on three processing steps including aerosol generation, thermal decomposition, and nanopowder collection. Such a system enables advanced synthetic method that provides control over particle size, morphology, nano/microstructure.

SPECIFICATIONS


System Structure



  •      • 
    Aerosol Generation: 2.4MHz Ultrasonic Enhanced Bubbler can
            "evaporate" catalyst liquid with literally no heat generated.
    A
            stainless steel liquid collector connects inline with the ultrasonic
            bubble can prevent condensing liquid from streaming into the
            furnace tube chamber.
  •      •  Thermal Decomposition: Tube Furnace can be heated up to
            1800C maximum. Bypassing the droplets flux across the
             temperature and atmosphere regulated firing zone, chemical, and
             physical conversion processes proceed.  
  •      •  Nanopowder Collection: 50KV, 2'' O.D tubular designed
            electrostatic precipitator (1.2L)can effectively collect nano-size
            particles from the carrier gas flow


Tube Furnace -

Thermal Decomposition





Voltage & Power

  •      •  Single Phase, 208V~240V AC, 50/60 Hz   (30A breaker required)
  •      •  Max. 2.5 KW


Working Temperature

  •      •  1750oC  continuous
  •      •  1800 oC  Max. < 1 hours
  •      •  1200oC, 1500oC, 1700oC furnace is available at lower cost

Max. Heating / Cooling Rate5oC / min ( T< 1600oC ); 2oC / min ( T>1600oC )

Heating Zone & Constant Temperature Zone

  •      •  12" total heating zone length
  •      •  3" ( +/- 1 oC )  constant heating zone

Heating Elements
 4 pcs Kanthal 1900ºC grade MoSi2 heating elements, made in Sweden

Temperature controller


  •      •  Eurotherm 3000 Series Programmable Temperature Controller.
  •      •  1 program, 24 segments programmed with ramping, cooling and
            dwelling steps
  •      •  Temperature Accuracy:  ±  0.1ºC


Laptop & software (Optional)

  •      •  Brand new laptop with Microsoft Window 10 and Microsoft Office
            2013 (30 days free trial) for immediate use.
  •      •  Labview Based Temperature Control System enables the user to
            edit temperature profile and manage heat-treatment recipe for MTI
             furnaces.
  •      •  Note: Due to the complexity of the controller operation, we
            strongly suggest customers purchase this PC control kit along
            with the furnace and our engineers will have the software &
            hardware pre-installed.



Processing Tube

  •      •  Premier grade high purity Al2O3 ceramic tube
     is included for
            operation @ 1500C~1800C. (I.
    D: 44mm x OD: 50 mm x 1200 mm
            length).
     Attention: carrier gas flow rate should be strictly
            controlled @ 100SCCM or less.

  •      •  Mullite tube (I.D: 44mm x OD: 50 mm x 1398 mm length) is included
             for continuous operation up to 1500C. Benefits from its high thermal
             shock resistivity, it can endure a max. carrier gas flows rate @
             200SCCM.


Sealing Flanges

& Fittings

  •      •  Left sealing flange with 1/4'' feedthrough, needle valve and
            mechanical pressure gauge. A 1/4'' O.D x 17'' L alumina tube is
            inserted into the main chamber. It can deliver the aerosol to the hot
             zone directly.
  •      •  Right KF50 quick disconnect flange provides direct coupling for the
             electrostatic precipitator.


            


Aerosol Generation

Utrasonic Enhanced Bubbler



  •      •  110VAC, 2.4 MHz Ultrasonic Generator
  •      •  Fluoropolymer coated liquid container and Fluoropolymer sealing
            gaskets
  •      •  external Fluoropolymer optical sensor and valve for keeping the
            liquid level to the correct height and preventing damage to the
            nebulizing element.
  •      •  Ultrasonic power programmable,0~100%, 5% increment.
  •      •  304 Stainless Steel T-piece (1.5'' sanitary fitting) with 1/4'' tube
            fitting adapters enables the use of carrier gas.



Mass Flow Controller




  • An MFC is employed to control the carrier gas flow rate.
    It is very important that the gas flow must be controlled <100SCCM in order to minimize the thermal shock impact on the furnace tube. 

Condensing Liquid Collector




  •      •  316 stainless steel made container, 150ml
  •      •  Two SS needle valves with 1/4" Tube Fittings
  •      •  The cap is attached to the body with a quick disconnect clamp.
            This allows for easy removal of components for cleaning



Nanopowder Collection

High Voltage Supply



  •      •  208~240VAC Single Phase, 15W max.
  •      •  Digital Voltmeter and Current meter, 50KV, 0.5mA max.
  •      •  Output voltage and current can be set by using knobs on the front
             panel and read from the digital display
  •      •  Constant current/Constant Voltage mode of operation
  •      •  Built-in Arc Protection Circuit


Tubular Electrostatic Precipitator

  •      •  Negative charged circular mesh plate and Positive charged 1''
            O.D x 170mmL Al tube collector are built into a transparent 2'' O.D
            x 450mm L-quartz tube
  •      •  The use of KF50 quick clamp and flange enables the quick coupling
             to the furnace processing tube
  •      •  Adjustable balance supports keep the collector leveled with the
            furnace tube
                     

Net Weight180Kg
Shipping Dimensions48"x40"x62"
Shipping Weight500 lbs
WarrantyOne year limited manufacturer warranty with lifetime support (consumable parts such as furnace liner, processing tubes, and O-rings are not covered by the warranty, please order replacements at related products below).

Compliance

     
 

  •      • 
    CE Certified
  •      •  NRTL (UL61010)  or CSA certification is available at extra cost. 

Application Notes



  •      • 
    Never use graphite crucible in the alumina tube.
  •      •  A two-stage pressure regulator must be installed on the gas     
            cylinder to limit the pressure to below 3 PSI for safe operation.
     
           Click here to learn the installation of a gas regulator.
  •      •  Never heat the furnace while the gas release valve is closed and
            a positive pressure condition exists within the furnace chamber.
            The pressure gauge must be used to closely monitor the chamber
             condition at all times during the heat
  •      •  The flow rate for gases should be limited to < 100 SCCM
            (alumina tube); <200SCCM (mullite tube)


Operation Instructions



         
                            
         Video: How To Set Up Furnace           How to create the
                                                                      Temperature gradient