CVD / PECVD Coating Furnace

Compact 1100ºC Tube Furnace with Solid Precursor Sublimator for CVD Growth of 2D Layers of TMDs - OTF-1200X-4-NW-UL

Compact 1100ºC Tube Furnace with Solid Precursor Sublimator for CVD Growth of 2D Layers of TMDs - OTF-1200X-4-NW-UL

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Product Name Compact 1100ºC Tube Furnace with Solid Precursor Sublimator for CVD Growth of 2D Layers of TMDs - OTF-1200X-4-NW-UL
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Product Code OTF1200XNW4
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Personalization

 
OTF-1200X-4-NW-UL is a compact 1100°C CVD tube furnace with precursor sublimating attachment. Totally four-channel gas inlets are built on the sublimation which allows feedings of various gases to carry the source vapor into the main heater for further decomposition and deposition. The sample holder fixture mounted on the right flange is slidable for easy sample loading/unloading. Such a system configuration is suitable for growing a wide range of transitional metal dichalcogenides (such as MoSe2, MoS2...) and wide bandgap semiconductors (such as h-BN) layers on substrate up to 3" diameter.

Specifications


Furnace and Preheater







  •      •  Compact CVD furnace system is modified from OTF-1200X-100 single zone tube furnace:
    •          º  Water cooling flange on left-side between the heater and furnace is used for
                   pre-heated gas input and sealing
  •      •  Four-channel gas inlet ( 1/8" Dia tube and tube fitting) are built-in on the left side flange
  •      •  One small heater is attached to the left side flange of the furnace to preheat input gas, liquid,
             or evaporate solid chemical, which will be then delivered to CVD furnace:
     
             Please click picture left for more details:
    •          º  1.2''O.D x 6''L SS tube as the heating chamber
    •          º  600ºC Max. working temperature
    •          º  Flange on the left side is for gas sealing and input

Rated VoltageSingle Phase, 220V AC, 50/60 Hz, AWG 8# Power cord is included (without plug)
Power consumptionMax. 3600 W (20 A breaker required)

Heating Zone

  •      •  CVD Furnace:  440 mm
  •      •  Constant temperature zone: 100 mm
  •      •  Gas Heater:     150mm




Working Temperature

  •      •  CVD Furnace:
    •          º  Max heating temperature: 1100°C ( < 2 hour )
    •          º  Continuous working temperature: 200~1000°C
    •          º  Max heating & cooling rate: 20°C/min

  •      •  Heater:
    •          º  Continuous working temperature: RT~600°C
    •          º  Max heating & cooling rate: 20°C/min


Temperature Control

   

  •      •  CVD Furnace and Heater (separate temp control):
    •          º  Digital controllers with PID/self-tuning functions and 30 segments programmable
    •          º  Thermocouple:  K type thermocouples, which feed through the right side flange and
                   control furnace temperature.
    •          º  Control accuracy: +/- 1°C
    •          º  RS485 Communications Port














Vacuum

and Gas Sealing & Flange
 

The right flange of CVD furnace
Left flange (between CVD Furnace and Heater) with four 1/8'' Swagelok fittings for 1/8'' tube:
  •      •  Two 1/8'' fitting on the flange for independently and directly delivering any gas into the
             CVD furnace
  •      •  One 1/8'' fitting for delivering heated gas from heater to CVD furnace
  •      •  One 1/4'' fitting for bypassing the gas (without heating) to the CVD furnace
            (inside the CVD furnace, the gas tube is merged with the heated gas pipe by a T fitting)
Note: How gas pipe assembled in the CVD furnace through above 1/8'' fitting:
  •      •  One 1/4'' quartz tube delivers the vapor gas from heater(also the bypass gas by a T fitting)
  •      •  Two 1/4'' quartz tube delivery extra gas via the two separate 1/8'' fitting on the big furnace left
             the flange
  •      •  These three 1/4'' quartz tubes inside CVD furnace is in parallel and vertically 1'' higher than
             sample holder
  •      •   These three 1/4'' quartz tubes can be easily removed to clean or replaced once get stuck
             or corroded
Heater:
  •      •  Left flange: one 1/8'' gas fitting to deliver gas to the heater for pre-heating and then to
            CVD furnace
     
  •      •  On the right side to CVD furnace with necessary thermal block material to minimize the
            temperature gradient at the interface between the heater and CVD furnace
  •      •  Furnace Chamber Installation
  •      •  2- 1/4" pipe adapter is installed on each flange


The optional Liquid Injection device

For direct liquid CVD  ( DLCVD), you may consider below devices for liquid injection: ( click Pic to order )

                            

Net weight
110kg

Dimensions




  •      •  Standard:    62"L X 18"W X 23"H
  •      •  Maximum:   80"L X 18"W X 32"H  (Lid open and right-side flange slided out)

Warranty


  •      •  One year limited warranty for electrical parts. ( Consumable parts such as processing tubes,
            o-rings and etc are not covered by the warranty)
  •      •  You may order replacement quartz tube here:  EQ-QZTube-SF


Laptop, software & WiFi Control (Optional)f

  •      •  Brand new laptop with Microsoft Window 10 and Microsoft Office 2013 (30 days free trial)
            for immediate use.
  •      •  Labview Based Temperature Control System (EQ-MTS01) enables the user to edit
            temperature profile, manage heat-treatment recipe, record and plot data for MTI furnaces.
  •      •  A wireless remote control provides up to 300 meters operating range.
  •      •  Above features are available upon request at an extra cost (up to $1,000). Please contact
            us for more information.
  •      •  Note:  The software is only compatible with MTI’s Yudian Temperature Controller

  •            


Compliance

   

  •      •  CE Certified
  •      •  NRTL(UL61010)  or CSA certifications are available at extra cost. 


Warning


Click here to learn the installation of a gas regulator


  •      •  The tube furnaces with quartz tube are designed for use under vacuum and low pressure
            <
    0.2 bars
  •      •  Attention: A two-stage pressure regulator must be installed on the gas cylinder to limit
            the pressure to below 3 PSI for safe operation.
     
    Click here to learn the installation of a gas
           regulator
    .
  •      •   Vacuum pressures may only be safely used up to 1000°C
  •      •  The flow rate for gasses should be limited to< 200ml/min) for reducing thermal shocks to the
             tube


Operation Demo Video & Instructions